Applied sciences

Chemical and Process Engineering

Content

Chemical and Process Engineering | 2020 | vol. 41 | No 4 |

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Abstract

The aim of the research presented in this paper was to determine the effect of vessel scale on gas hold- up in gas-liquid systems. The agitated vessel with internal diameters of T = 0:288 m and T = 0:634 m was filled with a liquid up to the height H = T. For the purpose of measurements, two high-speed impellers were used: Rushton turbine impeller (RT) or A 315 impeller.Within the study, the following parameters were altered: superficial gas velocity, impeller speed, impeller type and concentration of aqueous sucrose solution. In addition, influence of the vessel scale on gas hold-up value was analysed. Experimental results were mathematically described. Equations (5)–(7) do not have equivalents in the literature.
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Authors and Affiliations

Magdalena Cudak
1

  1. West Pomeranian University of Technology, Szczecin, Faculty of Chemical Technology and Engineering, al. Piastów 42, 71-065 Szczecin, Poland
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Abstract

In this study, we performed the qualitative analysis of exoproteins during granule formation in the pres- ence or in the absence of cations. The staining of thin granule cryosections showed that nucleic acids, proteins, polysaccharides and calcium cations were the dominant components of the granules. Proteins are the structural components associated with calcium ions. We determined changes in the proteomic profile and tightly bound extracellular polymeric substances (EPS) of the slime. The exopolymeric matrix containing the proteins was extracted using the Dowex resin method. Proteomic profile was analysed by SDS-PAGE method (sodium dodecyl sulphate polyacrylamide gel electrophoresis) using Coomassie blue staining in the samples of the aerobic granule matrix formed in the presence of multivalent cations and compared with that of the aerobic granules cultivated without cations. The results indicate that the granule matrix is predominantly composed of large and complex proteins that are tightly bound within the granular structure. The tightly bound extracellular polymeric substances (TB-EPS) may play a role in improved mechanical stability of aerobic granules. In the supernatant fraction of the sludge, only a small amount of free proteins in the medium molecular mass range was detected. The protein with high molecular mass ( 116 kDa) produced in the reactors with added Ca2+. Ca2+ had a considerable regulatory influence on production of extracellular proteins during aerobic granulation.
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Authors and Affiliations

Beata Kończak
1
Korneliusz Miksch
2

  1. Department ofWater Protection, Central Mining Institute, Pl. Gwarków 1, 40-166 Katowice, Poland
  2. Silesian University of Technology, Faculty of Energy and Environmental Engineering, Environmental Biotechnology Department, ul. Akademicka 2, 44-100 Gliwice, Poland
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Abstract

The study aimed to produce nano- and microfibrous materials from polyurethane (ChronoFlex®C75A/ C75D in 1,1,1,3,3,3–hexafluoro–2–propanol) by solution blow spinning. Experiments were carried out in order to determine the impact of solution blow spinning parameters on fibre diameter and quality of produced materials. The following properties of produced fibre scaffolds were investigated: fibre size, porosity and pore size, wettability, and mechanical properties. The results confirmed that produced nano- and microfibrous materials could be potentially used as scaffolds in three-dimensional cell and tissue cultures.
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Authors and Affiliations

Iwona Łopianiak
1
Michał Wojasiński
1
Beata Butruk-Raszeja
1

  1. Warsaw University of Technology, Faculty of Chemical and Process Engineering, Waryńskiego 1, 00-645 Warsaw, Poland
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Abstract

Thermoelectric generators using the Seebeck effect to generate electricity are increasingly used in various areas of human activity, especially in cases where a cheap high-temperature heat source is available. Despite many advantages, TEG generators have one major disadvantage: very low efficiency of heat conversion into electrical power which strongly depends on the applied load resistance. There is a maximum of generated power between the short and the open circuit in which it is zero. That is why optimization of TEG modules is particularly important. In this paper a method of maximization of generated power in a single TEG module is presented for two cases. The first case concerns a problem with fixed heat flux flow into the hot side of the module whereas the second one concerns a problem with fixed heat transfer parameters in hot heat exchanger i.e. supply gas temperature and heat transfer coefficient. A number of optimization results performed for various values of these parameters are presented and discussed.
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Authors and Affiliations

Artur Poświata
1
Paweł Gierycz
1

  1. Warsaw University of Technology, Faculty of Chemical and Process Engineering, ul. Waryńskiego 1, 00-645 Warsaw, Poland
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Abstract

Kinetic studies of esterification reaction of maleic anhydride with butan-1-ol, 2-methylpropan-1-ol and butan-2-ol were carried out in a semibatch reactor, in the presence of four acidic catalysts: sulfuric acid, phosphotungstic acid, ion exchange resin Dowex 50WX8 and tetrabutyl zirconate. Phosphotungstic acid proved to be the most active catalyst. The temperature range was 383–413 K, the initial molar ratio of alcohol to acid ranged 2.2-5:1. The kinetic parameters were given. The kinetics appeared to be that of the second order with respect both to the acid and to the alcohol. The reaction carried out in the presence of tetrabutyl zirconate was very slow and depended only on acid concentration. The effect of temperature on the reaction rate follows the Arrhenius equation well.
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Authors and Affiliations

Maria Bartoszewicz
1
Maria Kulawska
2
Wiesław Organek
2

  1. Łukasiewicz Research Network – Institute of Heavy Organic Synthesis “Blachownia”, Energetyków 9, 47-225 Kędzierzyn-Koźle, Poland
  2. Polish Academy of Sciences, Institute of Chemical Engineering, Bałtycka 5, 44-100 Gliwice, Poland

Instructions for authors

All manuscripts submitted for publication in Chemical and Process Engineering must comprise a description of original research that has neither been published nor submitted for publication elsewhere.

The content, aim and scope of the proposals should comply with the main subject of the journal, i.e. they should deal with mathematical modelling and/or experimental investigations on momentum, heat and mass transfer, unit processes and operations, integrated processes, biochemical engineering, statics and kinetics of chemical reactions. The experiments and modelling may cover different scales and processes ranging from the molecular phenomena up to production systems. The journal language is grammatically correct British English.

Chemical and Process Engineering publishes: i) full text research articles, ii) invited reviews, iii) letters to the editor and iv) short communications, aiming at important new results and/or applications. Each of the publication form is peer-reviewed by at least two independent referees.  

Submission of materials for publication

The manuscripts are submitted for publication via e-mail address office.cpe@pw.edu.pl. When writing the manuscript, authors should preferably use the template for articles. 

Proposals of a paper should be uploaded using the Internet site of the journal and should contain:

  • a manuscript file in Word format (*.doc, *.docx),
  • the manuscript mirror in PDF format,
  • all graphical figuresin separate graphics files.

In the following paragraphthe general guidelines for the manuscript preparation are presented.

Manuscript outline

        1. Header details
          1. Title of paper
          2. Names (first name and further initials) and surnames of authors
          3. Institution(s) (affiliation)
          4. Address(es) of authors
          5. Information about the corresponding author; academic title, name and surname, email address, address for correspondence
        2. Abstract – should contain a short summary of the proposed paper. In the maximum of 200 words the authors should present the main assumptions, results and conclusions drawn from the presented study.
        3. Keywords– Up to 5 characteristic keyword items should be provided.
        4. Text
          1. Introduction. In this part, description of motivation for the study and formulation of the scientific problem should be included and supported by a concise review of recent literature.
          2. Main text. It should contain all important elements of the scientific investigations, such as presentation of experimental rigs, mathematical models, results and their discussion. This part may be divided into subchapters.
          3. Conclusions. The major conclusions can be put forward in concise style in a separate chapter. Presentation of conclusions from the reported research work accompanied by a short commentary is also acceptable.
          4. Figures: drawings, diagrams and photographs can be in colour and should be located in appropriate places in the manuscript text according. Their graphical form should be of vector or raster type with the minimum resolution of 900 dpi. In addition, separate files containing each of the drawings, graphs and photos should be uploaded onto the journal Web site in one of the following formats: bmp, gif, tiff, jpg, eps. Due to rigid editorial reasons, graphical elements created within MS Word and Excel are not acceptable. The final length of figures should be intended typically for 8 cm (single column) or 16 cm in special cases of rich-detail figures. The basic font size of letters in figures should be at least 10 pts after adjusting graphs to the final length.  

          Figures: drawings, diagrams and photographs should be in gray scale. In case of coloured graphs or photo an additional payment of 300 PLN (72 €) per 1 page containing coloured figures on both sides, or 150 PLN (36 €) per page containing coloured figures on one side will be required.

          Tables should be made according to the format shown in the template.

        5. All figures and tables should be numbered and provided with appropriate title and legend, if necessary. They have to be properly referenced to and commented in the text of the manuscript.

        6. List of symbols should be accompanied by their units
        7. Acknowledgements may be included before the list of literature references
        8. Literature citations

 

The method of quoting literature source in the manuscript depends on the number of its authors:

  • single author – their surname and year of publication should be given, e.g. Marquardt (1996) or (Marquardt, 1996),
  • two authors – the two surnames separated by the conjunction “and” with the publication year should be given, e.g. Charpentier and McKenna (2004) or (Charpentier and McKenna, 2004),
  • three and more authors – the surname of the first author followed by the abbreviation “et al.” and year of publication should be given, e.g. Bird et al. (1960) or (Bird et al., 1960).

In the case of citing more sources in one bracket, they should be listed in alphabetical order using semicolon for separation, e.g. (Bird et al., 1960; Charpentier and McKenna, 2004; Marquardt, 1996). Should more citations of the same author(s) and year appear in the manuscript then letters “a, b, c, ...” should be successively applied after the publication year.

Bibliographic data of the quoted literature should be arranged at the end of the manuscript text in alphabetic order of surnames of the first author. It is obligatory to indicate the DOI number of those literature items, which have the numbers already assigned. Journal titles should be specified by typingtheir right abbreviationsor, in case of doubts, according to the List of Title Word Abbreviations available at http://www.issn.org/2-22661-LTWA-online.php.

Examples of citation for:

Articles
Charpentier J. C., McKenna T. F., 2004.Managing complex systems: some trends for the future of chemical and process engineering. Chem. Eng. Sci., 59, 1617-1640. DOI: 10.1016/j.ces.2004.01.044.

Information from books (we suggest adding the page numbers where the quoted information can be found)
Bird R. B., Stewart W.E., Lightfood E.N., 2002. Transport Phenomena. 2nd edition, Wiley, New York, 415-421.

Chapters in books
Hanjalić K., Jakirlić S., 2002. Second-moment turbulence closure modelling, In: Launder B.E., Sandham N.D. (Eds.), Closure strategies for turbulent and transitional flows. Cambridge University Press, Cambridge, 47-101.

Conferences
ten Cate A., Bermingham S.K., Derksen J.J., Kramer H.M.J., 2000. Compartmental modeling of an 1100L DTB crystallizer based on Large Eddy flow simulation. 10th European Conference on Mixing. Delft, the Netherlands, 2-5 July 2000, 255-264.


Suggested Reviewers

Authors are kindly requested to include a list of 3 potential reviewers for their manuscript, with complete contact information. These reviewers must not be from the authors' institutions, or have co-authored with authors of the manuscript.

Payments

Starting from 2014 a principle of publishing articles against payment is introduced, assuming non-profit making editorial office. According to the principle authors or institutions employing them, will have to cover the expenses amounting to 40 PLN (or 10 €) per printed page. The above amount will be used to supplement the limited financial means received from the Polish Academy of Sciences for the editorial and publishing; and in particular to increase the capacity of the next CPE volumes and to proofread the linguistic correctness of the articles. The method of payment will be indicated in an invoice sent to the authors or institutions after acceptance of their manuscripts to be published. In justifiable cases presented in writing, the editorial staff may decide to relieve authors from basic payment, either partially or fully. All correspondence should be sent to Executive Editor: dr hab. inż. Paweł Sobieszuk, email address: office.cpe@pw.edu.pl


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