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Number of results: 43
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Abstract

The paper presents the use of rapid prototyping technology of three dimensional printing (3DP) to make a prototype shell casting mold. In the first step, for identification purposes, a mold was prepared to enable different alloys to be cast. All molds being cast were designed in a universal CAD environment and printed with the zp151 composite material (Calcium sulfate hemihydrate) with a zb63 binder (2- pyrrolidone). It is designated to be used to prepare colourful models presenting prototypes or casting models and molds. The usefulness of 3DP technology for use with copper alloys, aluminum and zinc was analyzed. The strength of the mold during casting was assumed as a characteristic comparative feature in the material resistance to high temperature, the quality of the resulting casting and its surface roughness. Casting tests were carried out in vacuum – pressure casting. The casting programs applied, significantly increased the quality of castings and enabled precise mold submergence. Significant improvement was noted in the quality compared to the same castings obtained by gravity casting.
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Abstract

The study presents the results of the investigations of the effect of Cu, Ni, Cr, V, Mo and W alloy additions on the microstructure and mechanical properties of the AlSi7Mg0.3 alloy. The examinations were performed within a project the aim of which is to elaborate an experimental and industrial technology of producing elements of machines and devices complex in their construction, made of aluminium alloys by the method of precision investment casting. It was demonstrated that a proper combination of alloy additions causes the crystallization of complex intermetallic phases in the silumin, shortens the SDAS and improves the strength properties: Rm, Rp0.2,HB hardness. Elevating these properties reduces At, which, in consequence, lowers the quality index Q of the alloy of the obtained casts. Experimental casts were made in ceramic moulds preliminarily heated to 160 °C, into which the AlSi7Mg0.3 alloy with the additions was cast, followed by its cooling at ambient temperature. With the purpose of increasing the value of the quality index Q, it is recommended that the process of alloy cooling in the ceramic mould be intensified and/or a thermal treatment of the casts be performed (ageing)(T6).
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Abstract

The work presents the test result of the influence of cooling rate on the microstructure of AZ91 alloy, Vickers micro-hardness and Brinell hardness. Studies cooling and crystallization of AZ91 alloy was cast into the ceramic shells pre-heated to 180 ° C and then air-cooled at ambient temperature or intensively super cooled in the liquid coolant. The TDA method was applied to record and characterize the thermal effect resulting from the phase transformations occurring during the crystallization of AZ91 alloy. The kinetics and dynamics of the thermal processes of crystallization of AZ91 alloy in the ceramic shells were determined. Metallographic tests were performed with the use of an optical microscope. A comparison of these test results with the thermal effect recorded by way of the TDA method was made. Influence of cooling rate of AZ91 on HV0, 01 micro-hardness and Brinell hardness alloy was examined.
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Abstract

The work deals with the influence of change in the filling conditions of the ceramic moulds with plaster binder on the presence of gaseous porosity and the microstructure of the achieved test castings with graded wall thickness. Castings made of EN AC-44000 alloy, produced either by gravity casting, or by gravity casting with negative pressure generated around the mould (according to the Vacumetal technology), or by counter-gravity casting were compared. The results of examinations concerning the density of the produced castings indicate that no significant change in porosity was found. The increased size of silicon crystals was found for the increased wall thicknesses due to the slower cooling and solidification of castings.
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Abstract

The performed examinations concerning the process of filling the plaster ceramic moulds with aluminium alloys allowed to assess the influence of various methods of introducing the metal into the mould cavity on the macro- and microstructure of the obtained experimental castings. The comparison was performed for castings with graded wall thickness made either of EN AC-44000 alloy or of EN AC-46000 alloy, produced either by gravity casting, or by gravity casting with negative pressure generated around the mould (according to the Vacumetal technology), or by counter-gravity casting. It was found that the silicon crystals grow in size with an increase in wall thickness due to the slower cooling and solidification of castings.
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Abstract

The study discusses the issues connected with the production of thin-walled ceramic slurry in the replicast cs technology. In the ceramic mould production process, a special role is played by the liquid ceramic slurry used to produce the first layer of the mould. The study examines selected technological properties of liquid ceramic slurries used to produce moulds in the replicas cs technology. The ceramic slurries for the tests were prepared based on the binders Ludox Px30 and Sizol 030, enriched with Refracourse flour. The wettability of the pattern's surface by the liquid ceramic slurry and the dependence of the apparent viscosity on the ceramic flour content in the mixture were determined. The wettability of the pattern surface by the liquid ceramic slurry was determined based on the measurement of the wetting angle. The angle was determined by means of an analysis of the computer image obtained with the use of a CDC camera.
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Abstract

Paper presents the results of ATD and DSC analysis of two superalloys used in casting of aircraft engine parts. The main aim of the research was to obtain the solidification parameters, especially Tsol and Tliq, knowledge of which is important for proper selection of casting and heat treatment parameters. Assessment of the metallurgical quality (presence of impurities) of the feed ingots is also a very important step in production of castings. It was found that some of the feed ingots delivered by the superalloy producers are contaminated by oxides located in shrinkage defects. The ATD analysis allows for quite precise interpretation of first stages of solidification at which solid phases with low values of latent heat of solidification are formed from the liquid. Using DSC analysis it is possible to measure precisely the heat values accompanying the phase changes during cooling and heating which, with knowledge of phase composition, permits to calculate the enthalpy of formation of specific phases like γ or γ′.
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Abstract

Paper presents the results of research on modified surface grain refinement method used in investment casting of hollow, thin-walled parts made of nickel based superalloys. In the current technology, the refining inoculant is applied to the surface of the wax pattern and then, it is transferred to the ceramic mould surface during dewaxing. Because of its chemical activity the inoculant may react with the liquid metal which can cause defects on the external surface of the cast part. The method proposed in the paper aims to reduce the risk of external surface defects by applying the grain refiner only to the ceramic core which shapes the internal surface of the hollow casting. In case of thin-walled parts the grain refinement effect is visible throughout the thickness of the walls. The method is meant to be used when internal surface finish is less important, like for example, aircraft engine turbine blades, where the hollowing of the cast is mainly used to lower the weight and aid in cooling during operation.
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Abstract

The paper presents results of calorimetric studies of foundry nickel superalloys: IN100, IN713C, Mar - M247 and ŻS6 U. Particular attention was paid to determination of phase transiti ons temperatures during heating and cooling. The samples were heated to a temperature of 1500°C with a rate of 10°C ⋅ min – 1 and then held at this temperature for 5 min. After a complete melting, the samples were cooled with the same rat e. Argon with a purity of 99.99% constituted the protective atmosphere. The sample was placed in an alundum crucible with a capacity of 0.45 cm 3 . Temperature and heat calibration was carried out based on the mel ting point of high- purity Ni. The tests were carried out by the differential scanning calorimetry (DSC) using a Multi HTC high -temperature calorimeter from Setaram. Based on the DSC curves, the following temperatures were determined: solidus and liquidus, dissolution and precipitation of the γ ’ phase, MC carbides and melting of the γ ’ /γ eutectic. In the temperature range of 100 -1100°C, specific heat capacity of the investigated superalloys was determined. It was found that the IN713C and IN100 alloys exhibit a higher specific heat while compared to the Mar - M247 and ŻS6 U alloys.
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Abstract

The paper presents the results of studies on the development of correlation of solidification parameters and chemical composition of nickel superalloy IN-713C, which is used i.a. on aircraft engine turbine blades. Previous test results indicate significant differences in solidification parameters of the alloy, especially the temperatures Tliq and Tsol for each batch of ingots supplied by the manufacturer. Knowledge of such a relationship has important practical significance, because of the ability to asses and correct the temperatures of casting and heat treatment of casts on the basis of chemical composition. Using the statistical analysis it was found that the temperature of the solidification beginning Tliq is mostly influenced by the addition of carbon (similar to iron alloys). The additions of Al and Nb have smaller but still significant impact. Other alloying components do not have significant effect on Tliq. The temperature Teut is mostly affected by Ni, Ti and Nb. The temperature Tsol is not in any direct correlation with the chemical composition, which is consistent with previous research. The temperature Tsol depends primarily on the presence of non-metallic inclusions present in feed materials and introduced during the melting and casting processes.
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Abstract

The study involved using the liquid-solid compound casting process to fabricate a lightweight ZE41/AlSi12 bimetallic material. ZE41 melt heated to 660 oC was poured onto a solid AlSi12 insert placed in a steel mold. The mold with the insert inside was preheated to 300 oC. The microstructure of the bonding zone between the alloys was examined using optical microscopy and scanning electron microscopy. The chemical composition was determined through linear and point analyses with an energy-dispersive X-ray spectroscope (EDS). The bonding zone between the magnesium and aluminum alloys was about 250 μm thick. The results indicate that the microstructure of the bonding zone changes throughout its thickness. The structural constituents of the bonding zone are: a thin layer of a solid solution of Al and Zn in Mg and particles of Mg-Zn-RE intermetallic phases (adjacent to the ZE41 alloy), a eutectic region (Mg17(Al,Zn)12 intermetallic phase and a solid solution of Al and Zn in Mg), a thin region containing fine, white particles, probably Al-RE intermetallic phases, a region with Mg2Si particles distributed over the eutectic matrix, and a region with Mg2Si particles distributed over the Mg-Al intermetallic phases matrix (adjacent to the AlSi12 alloy). The microstructural analysis performed in the length direction reveals that, for the process parameters tested, the bonding zone forming between the alloys was continuous. Low porosity was observed locally near the ZE41 alloy. The shear strength of the AZ91/AlSi17 joint varied from 51.3 to 56.1 MPa.
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Abstract

Bimetallic AZ91/AlSi17 samples were produced by compound casting. The casting process involved pouring the AZ91 magnesium alloy heated to 650oC onto a solid AlSi17 aluminum alloy insert placed in a steel mould. Prior to casting, the mould with the insert inside was heated to about 370oC. The bonding zone formed between AZ91 and AlSi17 had a thickness of about 200 μm; it was characterized by a non-homogeneous microstructure. Two different areas were distinguished in this zone: the area adjacent to the AZ91 and the area close to the AlSi17. In the area closest to the AZ91 alloy, a eutectic composed of an Mg17Al12 intermetallic phase and a solid solution of Al in Mg was observed. In bonding zone at a certain distance from the AZ91 alloy an Mg2Si phase co-occurred with the eutectic. In the area adjacent to the AlSi17 alloy, the structure consisted of Al3Mg2, Mg17Al12 and Mg2Si. The fine Mg2Si phase particles were distributed over the entire Mg-Al intermetallic phase matrix. The microhardness of the bonding zone was much higher than those of the materials joined; the microhardness values were in the range 203-298 HV. The shear strength of the AZ91/AlSi17 joint varied from 32.5 to 36 MPa.
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Abstract

The herein paper contains the results of investigations on a new type of cellulose blend used for the manufacture of profiles applied in the process of making gating systems in the foundry industry. A standard cellulose profile was subjected to an experiment. During the experiment the profile was filled with a liquid cast iron and at the same time the temperatures of the liquid metal crystallizing inside the profile were measured as well as the temperature of the outer layer of the profile was controlled. Further, the microstructure of the cast iron, which crystallized out inside the cellulose profile, was analysed and the cellulose, thermally degraded after the experiment, was verified with the use of the chemical analysis method. Moreover, a quality analysis of the original as well as the degraded cellulose profile was run with the use of the FTIR infrared spectroscopy. The presented results revealed that the cellulose blend is aluminium silicate enriched and contains organic binder additives. The cast iron, which crystallized out, tended to have an equilibrium pearlitic structure with the release of graphite and carbides. The generation of disequilibrium ausferrite phases was also observed in the structure.
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Abstract

This article presents the results of studies in the hypoeutectic silumin destined for pressure die casting with the simultaneous addition of chromium and tungsten. The study involved the derivative and thermal analysis of the crystallization process, metallographic analysis and mechanical properties testing. Silumin 226 grade was destined for studies. It is a typical silumin to pressure die casting. AlCr15 and AlW8 preliminary alloys were added to silumin. Its quantity allowed to obtain 0.1, 0.2, 0.3 and 0.4% of Cr and W in the tested alloy. Studies of the crystallization process as well as the microstructure of the silumin poured into DTA sampler allowed to state the presence of additional phase containing 0.2% or more Cr and W. It has not occurred in silumin without the addition of above mentioned elements. It is probably the intermetallic phase containing Cr and W. DTA studies have shown this phase crystallizes at a higher temperature range than α (Al) solid solution. In the microstructure of each pressure die casting containing Cr and W the new phases formed. Mechanical properties tests have shown Cr and W additives in silumin in an appropriate amount may increase its tensile strength Rm (about 11%), the yield strength Rp0.2 (about 21%) and to a small extent elongation A.
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Abstract

The article presents the investigations of 7xxx aluminium alloys performed by the method of thermal and derivational analysis. The studies made it possible to identify the effect of the changes in the Cu concentration, the total Zn and Mg weight concentrations and the Zn/Mg weight concentration ratio on their crystallization process: the cooling as well as the kinetics and dynamics of the thermal process of cooling and crystallization. Metallographic studies were performed on the microstructure of the examined alloys and their HB hardness was measured. The evaluation of the changes was presented in reference to the model alloys EN AW-7003 and EN AW-7010, whose microstructure under the conditions of thermodynamic equilibrium are described by the phase diagrams: Al-Zn-Mg and Al-Zn-Mg-Cu. The performed investigations confirmed that the hardness HB of the examined alloys is mainly determined by the reinforcement of the matrix αAl by the introduced alloy additions and the presence of phases Θ(Al2Cu) and S(Al2CuMg) rich in copper, as well as η(MgZn2), in the examined alloys' microstructure. The increase of the amount of intermetallic phases precipitated in the microstructure of the examined alloys is caused, beside Cu, by the characteristic change of Zn wt. concentration and Mg. It was proposed that the process of one-stage thermal treatment of the examined alloys be introduced at a temperature of up to tJ-20 °C, which will prevent the exceedance of the solidus temperature.
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Abstract

The work presents the results of the investigations of the effect of inhibitors coated on the internal walls of a ceramic mould on the quality of the obtained casts made of the AM60 alloy containing additions of chromium and vanadium. In order to reduce the reactivity of magnesium alloy cast by the technology of investment casting with the material of the mould and the ambient atmosphere, solid inhibitors were applied in the form of a mixture of KBF4 and H3BO3 after the stage of mould baking and before the mould’s being filled with the liquid alloy. For the purpose of examining the effect of the inhibitors on the surface quality of the obtained casts, profilometric tests were performed and the basic parameters describing the surface roughness, Ra, Rz and Rm, were determined.
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Abstract

The paper presents the results of research on the determination of the effect of pouring temperature on the macrostructure of the castings subjected to complex (surface and volume) modification and double filtration. Tested castings were made of post-production scrap (gating system parts) of IN-713C superalloy. Tests included the evaluation of the number of grains per 1 mm2 , mean grain surface area, shape factor and tensile strength. Casting temperature below 1470 °C positively influenced the modification effect. The grains were finer and the mechanical properties increased, especially for castings with thicker walls. On the other hand, manufacture of thin walled castings of high quality require pouring temperature above 1480 °C.
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Abstract

In current casting technology of cored, thin walled castings, the modifying coating is applied on the surface of wax pattern and, after the removal of the wax, is transferred to inner mould surface. This way the modification leading to grain refinement occur on the surface of the casting. In thin walled castings the modification effect can also be seen on the other (external) side of the casting. Proper reproduction of details in thin walled castings require high pouring temperature which intensify the chemical reactions on the mould – molten metal interface. This may lead to degradation of the surface of the castings. The core modification process is thought to circumvent this problem. The modifying coating is applied to the surface of the core. The degradation of internal surface of the casting is less relevant. The most important factor in this technology is “trough” modification – obtaining fine grained structure on the surface opposite to the surface reproduced by the core.
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Abstract

The development of economy and industry introducing new technologies and materials often means the increased threat of occurrence of factors harmful to humans and environment. Workers employed in foundries as mould pourers are the group of high professional risk. Foundry moulding sands when poured with liquid metal are a source of the emission of harmful, toxic and carcinogenic (benzene, PAHs) compounds. The paper presents the results of studies on the concentration of chemical compounds emitted in the process of casting aluminium alloy and brass using moulding sands with the new inorganic binders. The specific values of the exposure indices were compared with the limit values. This enabled an assessment of the impact of moulding sands on work environment. The obtained results were compared with the values of contaminants emitted when pouring foundry moulds made from furan sands and bentonite sands with an addition of coal dust. Studies were carried out under the project POIG.01.01.02-00-015/09 "Advanced materials and technologies."
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Abstract

The paper analyses specific defects of castings produced by semi-solid casting process, especially rheocasting method SEED, which uses mechanical swirling for reaching proper structure in semisolid state with high content of solid fraction. Heat treated alloy AlSi7Mg0.3 was applied for producing an Engine Bracket casting part. For observing structure, metallographic observation by light and SEM microscopy was used. To analyse the process, software ProCAST was used to simulate the movements in shot chamber and filling of the mold.
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Abstract

The aging granulate is to activate the blowing agent during the manufacturing process to granulate models can re-expand and shape the model of well-sintered granules, smooth surface and a suitable mechanical strength. The article presents the results of studies which aim was to determine the optimum time for aging pre-foamed granules for pre-selected raw materials. The testing samples were shaped in an autoclave, with constant parameters sintering time and temperature. Samples were made at 30 minute intervals. Models have been subjected to flexural strength and hardness.
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Abstract

In highly developed countries, a significant progress in the use of alternative and clean energy sources has recently been observed. The European Union has implemented a programme to build wind turbines. It is estimated that in the coming years, thanks to the support in tax and credit, the global energy will develop very intensively. Many components of the wind turbines are castings. The basic material used for these castings is ductile iron, which in this particular case must meet high requirements imposed by the operating conditions of wind turbines. Anticipating an increase in customer demand for this type of castings, Krakodlew SA has decided to modernize its foundry using the ability to obtain external financing. The ductile iron manufacturing technology is now being developed and adapted to the specific conditions of the foundry plant, including the melting process yielding cast material with the required chemical composition, the technology of moulding, and the conditions for possible secondary metallurgy, spheroidizing treatment and graphitizing inoculation. The fulfilment of the imposed conditions for the casting production demands the use of advanced casting technologies introduced to the manufacturing process. The development of technology to launch the production of ductile iron castings for the wind power industry was supported by The National Centre for Research and Development (NCBiR). This article presents part of research on the binding kinetics of furan resin sands and choice of their composition for moulds and cores to make heavy castings used as components of equipment for the wind power industry.
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Abstract

A special Slag-Prop Cu database has been developed to archive data from laboratory and industrial tests related to post-reduction slags. In order to enrich the data areas, it was decided to design a system for measuring the temperature of the liquid slag and its viscosity. Objectives of research work are to gather information on the properties of post-slags such as the temperature of liquid slag and its viscosity. The discussed issues are especially important in the foundry practice. Designed research stand and using of database applications can greatly facilitate the work of metallurgists, foundrymen, technologists and scientists. The viscosity measurement was developed and presented earlier. The author's analytical methodology was supplemented by a thyristor measuring system (described in the article). The system temperature measurement can be performed simultaneously in 3 ways to reduce the measurement error. Measurement of the voltage mV - using the Seebeck effect can be measured throughout the entire range of thermocouple resistance, up to 1300 °C. Direct temperature measurement ⁰C - measurement only below 1000 ⁰C. Additional measurement - the measurement can also be read from the pyrometer set above the bath. The temperature and the reading frequency depend on the device itself. The principle of measurement is that in a molten metal / slag crucible, we put a N-type thermocouple. The thermocouples are hung by means of a tripod above the crucible and placed in a crucible. The thermocouple is connected to a compensating line dedicated to this type of thermocouple. The cable is in turn connected to a special multimeter that has the ability to connect to a computer and upload results. Temperature measurement can be performed simultaneously in 3 ways to reduce the measurement error. The Sn-Pb alloy has been subjected to testing for proper operation of the device. In this foot should be observed the supercooling of the liquid, which initiates the crystallization process and in which latent heat begins to exude raising the temperature until the coagulation temperature is reached.
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Abstract

The new investigation method of a permeability of ceramic moulds applied in the investment casting technology, is presented in the paper. Some concepts of performing permeability measurements are shown. Investigations in which the influence of the solid phase fraction in the liquid ceramic moulding sand (LCMS) on a permeability of a multi-layer ceramic mould were performed and discussed. The permeability was estimated during two the most important stages of the technological process: in the first – after wax melting and in the second – after mould annealing. Also an influence of the matrix grain sizes (material for sprinkling) on a ceramic mould permeability was estimated.
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Abstract

The investigation results of the kinetics of binding ceramic moulds, in dependence on the solid phase content in the liquid ceramic slurries being 67, 68 and 69% - respectively, made on the basis of the aqueous binding agents Ludox AM and SK. The ultrasonic method was used for assessing the kinetics of strengthening of the multilayer ceramic mould. Due to this method, it is possible to determine the ceramic mould strength at individual stages of its production. Currently self-supporting moulds, which must have the relevant strength during pouring with liquid metal, are mainly produced. A few various factors influence this mould strength. One of them is the ceramic slurry viscosity, which influences a thickness of individual layers deposited on the wax model in the investment casting technology. Depositing of layers causes increasing the total mould thickness. Therefore, it is important to determine the drying time of each deposited layer in order to prevent the mould cracking due to insufficient drying of layers and thus the weakening of the multilayer mould structure.
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